3-(3-Chlorobenzyl)-1H-isochromen-1-one

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3-(3-Fluoro­benz­yl)-1H-isochromen-1-one

The asymmetric unit of the title compound, C(16)H(11)FO(2), contains two independent mol-ecules. The isochromene ring systems are planar and are oriented with respect to the fluoro-benzene rings at dihedral angles of 87.15 (3) and 87.85 (3)° in the two mol-ecules.

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3-(3-Bromo­benz­yl)-1H-isochromen-1-one

In the title compound, C(16)H(11)BrO(2), the isocoumarin ring system is planar (r.m.s. deviation = 0.015 Å) and subtends a dihedral angle of 88.90 (2)° with the bromo-benzene ring. In the crystal, mol-ecules are linked, forming a three-dimensional packing pattern involving C-H⋯O inter-actions, Br⋯O contacts [3.4734 (10) Å] and π-π stacking inter-actions with centroid-centroid distances ranging ...

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3-(3-Chloro­benz­yl)-1H-isochromen-1-one

The asymmetric unit of the title compound, C(16)H(11)ClO(2), a chemically synthesized isocoumarin, contains three independent mol-ecules. The benzopyran and benzene rings are approximately perpendicular to each other, forming dihedral angles ranging from 83.08 (14) to 87.43 (11)°. In the crystal structure, mol-ecules are linked by inter-molecular C-H⋯O hydrogen-bonding inter-actions, forming ch...

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3-(4-Methoxy­phen­yl)-1H-isochromen-1-one

The asymmetric unit of the title compound, C(16)H(12)O(3), contains two crystallographically independent mol-ecules. The isochromene ring system is planar (maximum deviation 0.024 Å) and is oriented at dihedral angles of 2.63 (3) and 0.79 (3)° with respect to the methoxy-benzene rings in the two independent mol-ecules.

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3-[(R)-3,3-Dichloro-2-hydroxy­prop­yl]-8-hydr­oxy-6-meth­oxy-1H-isochromen-1-one

The title compound, C(13)H(12)Cl(2)O(5), is an isocoumarin compound which has been isolated from the ethyl acetate extract of the fermentation broth of actinomycete Streptomyces sp. (V(4)) from the South China Sea. There are intra- and inter-molecular hydrogen bonds and halogen bonds [Cl⋯Cl = 3.434 (2) Å; C-Cl⋯Cl = 121.6°]. The intermolecular O-H⋯O hydrogen bonds link mol-ecules into chains alo...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2008

ISSN: 1600-5368

DOI: 10.1107/s1600536808030274